The mass of most ceramic sherds with the Popovsky Lug archaeological internet site is relatively small (commonly while in the choice of two–five g), and we could use only a little Portion of the sample for your elemental analysis. Our sampling approach for elemental analysis was depending on reducing a subsample of about 250–350 mg from the initial sherd, milling it to powder, and examining it employing spectral methods.
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Place mapping was completed with 20 µm pixel sizing and fifty ms dwell time; the sample chamber was retained at 25 mbar vacuum. Mapping was carried out in two sequential runs (so-named frames); the ultimate map is usually a sum of two frames. The samples were being epoxy-mounted and polished just before the analysis.
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